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alpha-germanone

 Last Update: 2022-06-10
 Source: Internet
 Author: User

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1 8 pipe

1 3 dimethylamylamine

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alpha-germanone

α-Cyperone

【Structural formula】

[Molecular formula and molecular weight] C ₁₅ H ₂₂ O; 218.

[Source] Synthesis

【Properties】Yellow liquid

This product is soluble in methanol , ethanol , ethyl acetate and chloroform

Refractive index (20°C): 1.

【Purity Check】

TLC

Eluent, dichloromethane - ethyl acetate - acetic acid (80:1:1)

Inspection of 2,4-dinitrophenylhydrazine solution, observation under sunlight and ultraviolet light (254nm)

Developing agent toluene-ethyl acetate (19:1)

Inspection of 2,4-dinitrophenylhydrazine solution, observation under sunlight and ultraviolet light (254nm)

Gas chromatography

Column AB-INNOWAX capillary column, 0.

Column temperature: starting temperature 60℃, ending temperature 180℃, heating rate 8℃/min

【Structural identification】249

2929, 2862, 1668, 1612, 1453, 1376, 1351, 1200, 1084, 1019, 888

EI-MS m/z: 219[M+H] ⁺

¹ H-NMR (CDCl ₃ ) δ: 4.

¹³ C-NMR (CDCl ₃ ) δ: 37.

【Storage】Dry and airtight

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