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    Home > Chemicals Industry > Chemical Technology > Determination of 60 semi-volatile organic compounds in soils and sediments by gas chromatography-mass spectrometry (2)

    Determination of 60 semi-volatile organic compounds in soils and sediments by gas chromatography-mass spectrometry (2)

    • Last Update: 2022-02-25
    • Source: Internet
    • Author: User
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    Six, analysis and testing

    (1) Instrument conditions (for reference only, can be adjusted appropriately according to the actual instrument)

    1.


    Injection port: temperature is 280℃, column flow rate is 1.


    2.


    Ion source: EI, ion source temperature 300℃, ionization energy 70eV, solution delay time: 3.


    (2) Calibration curve

    Prepare a standard series of more than 5 points (such as 1.


    Refer to Table 7-9 for the retention time qualitative and quantitative ions under reference instrument conditions


    Table 7-9 Retention time and qualitative and quantitative reference ions



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