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Six, analysis and testing
(1) Instrument conditions (for reference only, can be adjusted appropriately according to the actual instrument)
1.
Injection port: temperature is 280℃, column flow rate is 1.
2.
Ion source: EI, ion source temperature 300℃, ionization energy 70eV, solution delay time: 3.
(2) Calibration curve
Prepare a standard series of more than 5 points (such as 1.
Refer to Table 7-9 for the retention time qualitative and quantitative ions under reference instrument conditions
Table 7-9 Retention time and qualitative and quantitative reference ions
Related Links: Determination of 60 Semi-volatile Organic Compounds in Soil and Sediment Gas Chromatography-Mass Spectrometry (1)