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The high capabilities of capillary electrophoresis (CE) in separation and detection have been well recognized, and most chaptersof this book are devoted to carbohydrate analysis utilizing these capabilities. CE has other inherent advantages. One is thatit allows real-time observation of chemical as well as physical reactions occurring in a capillary. We have previously publisheda few articles on various techniques of in-capillary chemical derivatization and demonstrated the usefulness of these techniquesfor the analysis of biological substances (
1
–
3
) and now discuss physical interactions in a capillary.