French rose volatile oil

Extraction source: This product is the volatile oil composition of the rose-based French rose Rosa Gallica Lflower extracted, the total volatile oil content of 80%(main ingredients) Citronellol, content: 40%p style"style"text-style": center; "align" "French rose volatile oil" src"/uploads/allimg/1612/2-161221AGW4.jpg"style""style: 253px; Height: 75px; ."Orange florinerolscented lyol lemonolvanilla acid Vanillic acidcontent: 40%.s character) This product is a clear yellow to orange-yellow clear, transparent liquidSoluble in ether, chloroform, ethyl acetate, acetone, ethanol"Identification" take this product plus ether to make 05% solution for test fluidTake the standard cider, cilantro, cider alcohol, orange flower alcohol and other ether to make each containing 10 sl / ml solution for controlTake the French rose standard control of the medicinal 1.0g plus ether 30 ml, ultrasonic extraction 30 minutes, the filter cold wind blowing away ether, residue plus ethyl acetate 1 ml dissolved, as a control liquidTake the above three liquid each 8 sl, respectively, on the same silicone G board, a point two board(1) Oil ether-acetone-ethyl ethyl acetate (94:5:1) unfolded, sprayed 1% vanilla aldehyde sulfuric acid solution, hot wind show(2) n-hexane-ethyl acetate (9:1) is expanded, sprayed with 5% vanilla aldehyde sulfuric acid solution, hot wind blowingthe above two plates, the corresponding position of the standard speckle appears the same color spots, compared to the standard medicinal spots, the corresponding rate of 60%fat oil: take this product 1.0g plus ethanol 10 ml, shake well placed, no oil dropletsheavy metals: no more than 10 ppm (appendix IX.E)content determination: Gas chromatography (appendix VI.E) measurementchromatography condition column: capillary column 0.25mm x 30mcolumn temperature: program heating up, 35 degrees C - 8 degrees C / minute - 120 degrees C - 6 degrees C / minute - 220 degrees C (5 minutes)inlet temperature: 240 degrees Cdo not divert into the sampleopen the valve after 0.75 minutescarrier: N: Constant current modeflow rate: 11ml/minsample determination: take this product plus ether to make 5% solution, take 1 sl into the sample measurement, the normalization method to calculate the contentVolatile Oil Determination: The Volatile Oil Measurement (Appendix XD) is measured: Anti-depressant, anti-inflammatory, analgesic, blood lipid-loweringstorage is closed, cool and dry