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    Home > Active Ingredient News > Drugs Articles > How to properly install a small double-glazed reactor

    How to properly install a small double-glazed reactor

    • Last Update: 2020-11-18
    • Source: Internet
    • Author: User
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    The inner layer of the glass double-layer reactor can be put into the reactive solution medium to do a stirring reaction, the mezzanine can be connected to different sources of heat and cold (frozen liquid, hot water or hot oil) to do a circular heating or cooling reaction.
    In the setting of thermostat conditions, in the closed glass reactor, according to the requirements of use in the normal pressure or negative pressure conditions for stirring reaction, and can do the reaction solution reflow and distillation, is the modern fine chemical plant, biopharmaceutical and new materials synthesis of the ideal pilot, production equipment.
    1, open the packaging, according to the packing list to check whether the main parts of the machine is complete.
    2, the stainless steel tube and the fixing part are assembled according to the drawings.
    3, install the electrical box on top of the right rear pole and tighten the screws, plug in the seven-core plug.
    the vacuum meter is mounted on the left rear end and the screws can be tightened.
    4, according to the height of use, the kettle circular carrier is fixed to the pole slider, the kettle is placed on the carrier, the semi-circular hoop is used to secure the kettle neck inserted into the pole slider, close and tighten the fixing screws, when installing, pay attention to the reactor body vertical.
    5, the mixing rod is fixed to the ring clamp head of the motor spindle, the mixing rod rotates the bearing through the middle of the cover, tightens the special connector, and then adjusts the position of the motor, paying attention to vertical centrity.
    6, the slider on the pole is a fixed adjustment in different directions and high and low stainless steel multi-use clip.
    7, the bottle cap on the left side of the 40 standard mouth plug snake-type reflow condenser, the right 40 s mark for the filling port to connect the constant pressure funnel, the front 24 s marker for the intestion thermometer casing port, the hat rear for the 34 s mark for multi-functional spare port, the bottom with a discharge valve, the bottom of the kettle is the circulation liquid import and export.
    the lower port to connect the circulation liquid inlet, the upper port to the circulation liquid return port.
    8, the installation of glass instruments should be clean, the interfaces are applied with Vaseline to prevent the phenomenon of glass clinging, and then coated with vacuum fat to prevent air leakage.
    9, press the 10,000-way wheel fixing device, stirring, if the stirring is stable, the commissioning is good.
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