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4.
4.
Adjust the instrument according to the following conditions, allow appropriate changes according to different instruments, and obtain a suitable degree of separation
a.
h.
c.
d.
e.
f.
Injection volume: 0.
4.
Area normalization method
4.
Adjust the instrument according to the above regulations.
4.
4.
3.
4 Calculation of results
The content of 2-ethylhexanol X 1 , expressed by mass percentage, calculated according to formula (1):
In the formula: A — the peak area of 2-ethylhexanol in the sample , mm 2 ;
∑A i — the sum of peak areas of impurities in the sample, mm 2 ;
X 4 —The moisture content in the sample, %
.
Take the arithmetic average of the two parallel determinations as the result
.
4.
3.
5 Tolerance
The difference between the two parallel determination results is not more than 0.
15%
.
4.
3.
6 Detection limit
The minimum detection concentration is 0.
002%
.
Related Links: Industrial Octanol (2-Ethylhexanol) (2)