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    Home > Active Ingredient News > Drugs Articles > Instructions for use and installation of double-layer glass reactor

    Instructions for use and installation of double-layer glass reactor

    • Last Update: 2022-05-03
    • Source: Internet
    • Author: User
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    Instructions for use and installation of double-layer glass reactor The double-layer glass reactor is a new type of glass reactor which has been improved for many years on the basis of the single-layer multi-functional glass reactor, which realizes convenient high and low temperature, and Rapid heating, cooling requirements of the experimental process, is a modern laboratory, chemical, core material synthesis instrument
    .

    The following are the instructions for use and installation of the double-layer glass reactor.
    Let's understand together
    .

    Instructions for use of double-layer glass reactor ● Please read the entire contents of this manual thoroughly before installation, use, maintenance and inspection, and use it correctly
    .

    ● The power supply voltage is the same as that specified by this instrument
    .

    ● No-load operation is not suitable for high-speed operation.
    ● The life of the electrical box is greatly affected by the surrounding temperature and humidity
    .

    Please keep the governor and motor dry
    .

    ● Install the machine first, then wire it by a professional electrician and turn it on
    .

    The ground terminal must be grounded
    .

    The high temperature bath is connected to the air switch
    .

    ● Within 5 minutes after the power is turned off, electric shock may still occur due to the discharge of the inverter or capacitor
    .

       ● Pay attention to the impact damage to the glass by hard objects (watches, rings, belt buckles, etc.
    ) on your body during operation
    .

       ● Pay attention to the impact damage to the glass by hard objects (watches, rings, belt buckles, etc.
    ) on your body during operation
    .

       ● Be careful when connecting the vacuum tube and water tube, so as not to damage the human body by breaking the glass with excessive force
    .

       ● When it is necessary to use a high temperature circulating oil bath, pay attention to the damage caused by high temperature to the human body.
    I recommend using a heat-conducting oil (dimethicone oil, kinematic viscosity of 100) that is less harmful to the human body as a solvent
    .

    Special attention should be paid to the high temperature cycle, the circulating pump should be turned on first, and the temperature should be raised slowly under the condition that the thermally conductive solvent is circulated
    .

       Installation of the instrument: (Only for the reaction kettle below 5L, and a special person is required for installation above 5L) 1 After opening the package, check whether the main accessories of the machine are complete according to the packing list
    .

       2.
    Assemble the frame with the stainless steel tube and the fixing parts as shown in the attached picture
    .

       3.
    Install the electrical box on the right rear pole, tighten the screws, and insert the seven-pin plug
    .

    The vacuum gauge is installed on the left rear end, just tighten the screw
    .

       4.
    According to the height of use, fix the round bracket of the kettle on the vertical rod slider, put the kettle on the bracket, and use the semi-circular hoop to fix the neck of the kettle and insert it into the vertical rod slider respectively.
    After closing, tighten the fixing screws.
    When installing, note that the main body of the reactor is vertical
    .

       5.
    The stirring rod is fixed on the gear ring chuck of the main shaft of the motor.
    The stirring rod passes through the middle rotating bearing of the cover, tighten the connector, and then adjust the position of the motor, paying attention to the vertical concentricity
    .

       6.
    The slider on the pole is a stainless steel multi-purpose clip that can be fixed and adjusted in different directions and heights
    .

       7.
    The 40# standard port on the left of the bottle cap is inserted into a snake-type reflux condenser, the right 40# standard port is the feeding port to connect the constant pressure funnel, the 24# standard port in the middle and front is the thermometer sleeve port, and the back of the cap is the 34# standard port It is a multi-function spare port, with a discharge valve at the bottom, and the upper and lower parts of the kettle are the inlet and outlet of the circulating liquid
    .

    The lower port is connected to the circulating liquid, and the upper port is connected to the circulating liquid return port
    .

       8.
    Clean when installing glass instruments, apply Vaseline to each interface to prevent the glass from locking, and then apply vacuum grease to prevent air leakage
    .

    9.
    Press the universal wheel fixing device to stir.
    If the stirring is stable, it means that the debugging has been completed.
    The above is the introduction to the instructions for use and installation of the double-layer glass reactor.
    I believe you will have the corresponding information after reading Understood, I hope to be helpful to everyone
    .

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