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Procedure for determination of 14 quinolones residues in honey

 Last Update: 2021-09-19
 Source: Internet
 Author: User

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11.

(1) Chromatographic conditions

Chromatographic column: Inertsilph-35um150mm×2.

Table 11-10 Gradient elution conditions

(2) Mass spectrometry conditions

Ion source: electrospray ion source; scanning method: positive ion scanning; detection method: multi-reaction monitoring; electrospray voltage: 5500V; atomizing gas pressure: 0.

Table 11-11 Qualitative ion pair, quantitative ion pair, collision gas energy and collision cell outlet voltage of fourteen quinolones

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