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Phenylthiourea (phenylthiourea) phenylthio also known as carbamide, N- phenylthiourea, of formula C .
7 H .
8 N 2 S, molecular weight of 152.
21, the formula
1.
Product performance
White needle-like crystals; melting point 154℃, easily soluble in ethanol , soluble in 400 parts of cold water and 17 parts of hot water; slightly bitter taste; toxic
.
2.
Production principle
Aniline is obtained by first forming a salt with sulfuric acid and then performing an addition reaction with sodium thiocyanate
.
3.
Process flow
4.
Technical formula (kg/t)
5.
Main equipment
Glass-lined reaction pot, high tank, suction filter, drying oven
.
6.
Production process
First, 1600 kg of anhydrous chloroform was added to the glass-lined reactor, and 240 kg of aniline was added with stirring
.
In about 1h, put 134kg 98% sulfuric acid in a trickle, and control the temperature at 25-50℃
7.
Product Standard
8.
Product use
Used in the synthesis of dye intermediates 2-aminobenzothiazole, 3-methylbenzothiazole urea, etc.
; also used in the determination of copper, gold, mercury, palladium, platinum, silver, etc.
, for quantitative analysis of elements (N, S) Standard sample
.
9.
Safety measures
(1) The raw material aniline is highly toxic, and the solvent chloroform is toxic
.
The equipment should be airtight, the operator should wear labor protection equipment, and the workshop should be well ventilated
Strong (2) the toxicity of this product, oral rat the LD 50 3mgkg
.
Packed in iron drums, stored in a cool and ventilated place, and stored and transported in accordance with the regulations for toxic chemicals
Related links: Product standards and uses of sodium m-nitrobenzene sulfonate