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7.
Laboratory preparation method
Three-necked flask was added 104g 98% sulfuric acid and containing 68g% SO 20 is .
3 of fuming sulfuric acid
.
Cool to below 30℃, add 67g benzene dropwise within 1h, and control 50~55℃
8.
Product Standard
9.
Quality inspection
Content determination: Weigh about 2.
2g of the sample (weigh to 0.
0002g) in a 500mL Erlenmeyer flask, add 100mL of water, after dissolution, correct the temperature to 20℃, add 30mL of hydrochloric acid, add 7g of zinc powder in batches under stirring
.
After the addition, continue to stir for 30 minutes and filter
Where: V 1 ——The volume of sodium nitrite standard solution consumed by the sample, mL;
V 2 ——The volume of sodium nitrite standard solution used in blank, mL;
c——The molar concentration of sodium nitrate standard solution, mol/L;
G——The mass of the sample, g
.
10.
Product use
This product is a mild oxidant, used as a dyeing aid
.
It can protect the color and light when fabric printing or padding and steaming; when fabric is smelted and mercerized, it can prevent cutting and covering paste; when printing and dyeing, it can offset the effect of reducing substances
11.
Safety measures
(1) The raw material benzene is toxic and flammable, and nitric acid, concentrated sulfuric acid, and fuming sulfuric acid are highly corrosive.
The equipment should be closed, the operators should wear labor protection equipment, and the workshop should be well ventilated
.
(2) Packed in chemical fiber board barrel lined with plastic bag, stored in a cool, ventilated and dry place, storage period is two years
.
Store and transport in accordance with drug regulations