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    Home > Active Ingredient News > Drugs Articles > Structure and operation guide of glass reactor

    Structure and operation guide of glass reactor

    • Last Update: 2013-05-22
    • Source: Internet
    • Author: User
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    Glass reaction kettle is composed of kettle body, kettle cover, jacket, agitator, transmission device, shaft seal device, support, etc Generally, there are anchor type, paddle type, turbine type, propulsion type or frame type mixing forms When the height diameter ratio of the mixing device is large, multi-layer mixing paddles can be used, or optional according to the user's requirements And a jacket is arranged outside the kettle wall, or a heat exchange surface is arranged inside the reactor, or heat exchange can be carried out through the external circulation The heating methods include electric heating, hot water heating, heat-transfer oil circulation heating, far-infrared heating, external (internal) coil heating, etc the cooling methods are jacket cooling, coil cooling in the kettle, stirring paddles, etc The supporting seat has supporting type or ear type support, etc Gear reducer should be used when the rotating speed is more than 160 The number, specification or other requirements of opening can be designed and manufactured according to the user's requirements In order to facilitate the user's use, the operation guide of finishing glass reactor is as follows: 1 To react with different media in the glass reactor, it is necessary to first check whether the media corrodes the main material Special order shall be made for the chemical reaction with violent instantaneous reaction, large amount of gas or high temperature, inflammable and explosive, as well as the reaction with high pressure, high temperature or medium containing chloride ion and fluorine ion, which have serious corrosion on stainless steel! Except for the transparent glass for the kettle body and jacket, other materials are stainless steel or other metal materials 2 The liquid level of the reactor body shall not exceed 2 / 3 of the liquid level when the reaction medium is loaded! 3 It is strictly prohibited to dismantle the reactor under pressure when it is working or at the end! It is strictly prohibited to work under the condition of overpressure and overtemperature! 4 The jacket heat-transfer oil shall be heated When the heat-transfer oil is added, attention shall be paid not to mix water or other liquid into it, and the oil level of the heat-transfer oil shall be checked irregularly 5 If there is abnormal sound inside the isolation sleeve during operation, stop the machine and release the pressure, and check whether the mixing system has any abnormal condition Check the swing amount of the mixing shaft regularly If the swing amount is too large, replace the bearing or sliding shaft sleeve in time! 6 Connect the corresponding voltage according to the use voltage of the controller, single-phase 220 V, three-phase 380 V, and do not connect the live line and zero line of the controller reversely; Wiring work shall not be carried out in power transmission to prevent electric shock! In order to ensure the normal operation of the controller and personal safety of the staff, please connect the ground wire! The controller itself is not explosion-proof, so it should avoid oil, gas and other flammable and explosive environment 7 After the final reaction temperature of Zui is determined, it is not allowed to change the temperature setting value in the heating process, so as to avoid large temperature overshoot!
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