Which methods can improve the efficiency of double-glazed reactor.

Double-glazed reactor is designed for double-glazed, the inner layer into the reactive solution can do stirring reaction, the mezzanine can be through different sources of heat and cold (frozen liquid, hot water or hot oil) to do circular heating or cooling reaction.
In the setting of thermostat conditions, in the closed glass reactor, according to the requirements of use in the normal pressure or negative pressure conditions for stirring reaction, and can do the reaction solution reflow and distillation, is the modern fine chemical plant, biopharmaceutical and new material synthesis of the ideal pilot, production equipment.
in the process of double-glazed reactor work, what ways and means can improve its efficiency? First, insulation medium Because the mezzanine thickness in the middle of the double-layer glass reactor is small, therefore, the insulation performance is poor.
high temperature and low temperature process, the use of insulation materials are required to protect the body of the body.
the reactor body and the pipe of the guide fluid need to be wrapped in insulation material, and pay attention to the thickness of the insulation layer to ensure a better insulation effect.
, temperature control medium selection According to the desired reaction temperature, choose different properties of the temperature control medium, as the reaction heat transmission medium.
low temperature, choose ice ethanol bath, room temperature, choose water bath, high temperature, choose oil bath.
use low or high temperatures, pay attention to the selection of the right medium, the key is viscosity.
the viscosity of the medium, the circulation pump may not move, the media circulation effect is not good, can not achieve the desired temperature control effect.
to replace the high-power circulation pump, pressure into the medium pressure is too large, easy to damage the double-glazed reactor lining, reactor rupture.
usually manufacturers will also according to their own products, supporting the corresponding heating media for selection.
3, feeding precautions Double-glazed reactor for independent reaction shelf, unlike industrial reactor has a reaction bench, and reserved feeding port is small, therefore, the feeding process is more difficult.
double-glazed reactor disposable feeding amount should not be too large, according to the reaction temperature, reflow and pressure, evaluation, add appropriate amount of material.
general, should not exceed 2/3 of the kettle body.
, storage location double-glazed reactor as a reaction amplification test device, the volume is usually 50 - 150L, the volume of specific circumstances can be customized, therefore, the scale of the test can not be underestimated.
because the kettle body is made of glass, stainless steel is a stand and the feet are casters, the storage location needs to be carefully selected.
casters can be fixed with a foot buckle, but the stability is not strong.
, the storage pay attention to choose a flat place, flat, keep the mechanical mixing center and reactor consistent, otherwise easy to shake unstable, out of a safety accident.
double-glazed reactor body height of about 1.5m, plus straight on the condensation tube, the overall reactor is about 2m.
general floor-to-ceiling ventilation kitchen can not be placed, but must be placed in a well-ventilated location.
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