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2-hydroxy-3-naphthoyl-o-toluidide (2-hydroxy-3-naphthoyl-o-toluidide), also known as naphthol AS-D (naphtholAS-D), N-(3-hydroxy-2-naphthoyl-o-toluidide) ) O-toluidine, molecular formula is C 18 H 15 NO 2 , molecular weight is 277.
28, structural formula is
1.
Product performance
Beige powder; melting point 195~196℃; insoluble in water and soda ash, soluble in benzene and naphtha ; yellow in alkaline solution; toxic
.
2.
Production principle
2-Hydroxy-3-naphthoic acid forms a salt with soda ash and then dehydrated
.
Then, 2-hydroxy-3-naphthoate sodium (2,3-sodium) is condensed with o-toluidine under the catalysis of phosphorus trichloride , and the product is obtained by neutralization, desolvation, filtration and drying
3.
Process flow
4.
Technical formula (kg/t)
5.
Main equipment
Salt formation pot, condensation reaction kettle, distillation kettle, storage tank, filter, dryer