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Alpha-Terpineol
α-Terpineol
【Synonym】α-terpineol
【Structural formula】
[Molecular formula and molecular weight] C 10 H 18 O; 154.
[Source] Pinus tabulie formis Carr.
【Properties】Colorless and transparent liquid
This product is easily soluble in ethyl acetate
【Purity Check】
TLC
1.
Eluent petroleum ether (30 ~ 60 ℃) - ethyl acetate (17: 3)
Check 10% sulfuric acid ethanol , heat at 105°C until the color is clear, check under sunlight and ultraviolet light (365nm)
2.
Developing solvent cyclohexane - ethyl acetate (17:3)
Check 10% sulfuric acid ethanol , heat at 105℃ until the color is clear, check the gas chromatograph under sunlight and ultraviolet light (365nm)
Chromatographic column: DB-5 capillary column, 0.
Column temperature: starting temperature 60℃, ending temperature 200℃, heating rate 10℃/min
[Structural identification] 260,215
3300, 2890, 2860, 1440, 1380, 1370, 1140, 910, 840, 790
EI-MS m/z: 154[M] + , 136, 121, 93, 81, 59, 43, 28
1 H-NMR (CDCl 3 ) δ: 1.
13 C-NMR (CDCl 3 ) δ: 23.
【Storage】Dry, airtight, refrigerate and protect from light
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