Glycerol trioleate

Glycerol trioleate

Glyceryl trioleate

【Structural formula】

[Molecular formula and molecular weight] C ₅₇ H ₁₀₄ O ₆ ; 885.

[Source] Synthesis

【Properties】Colorless and transparent liquid

This product is easily soluble in chloroform and petroleum ether , but insoluble in water

【Purity Check】

TLC

1.

Eluent petroleum ether (60 ~ 90 ℃) - ether - acetic acid (10: 1 0.

Check 10% sulfuric acid ethanol solution, heat at 105℃ until the spots are clear, check under sunlight

2.

Developing agent petroleum ether (60～90℃) -ethyl acetate (10:1)

Check 10% sulfuric acid ethanol solution, heat at 105℃ until the spots are clear, check under sunlight

High performance liquid chromatography

Column HIQ-silC ₁₈ , 5pm (4.

Mobile phase acetonitrile- dichloromethane (60:40), 1ml/min

Evaporation light detector: drift tube temperature: 80℃

【Structural identification】201

2925, 2854, 1747, 1458, 1163

ESI-MS m/z: 903[M+NH4] ⁺ , 754, 681, 604

¹ H-NMR (CDCl ₃ ) δ: 5.

¹³ C-NMR (CDCl ₃ ) δ: 173.

【Storage】Dry and airtight

Related link: carvesol