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Appendix A
(Standard appendix)
Typical chromatogram
A1 Method two determination of dimethylamine aqueous solution typical chromatogram
A typical chromatogram of dimethylamine aqueous solution is shown in Figure A1
Figure A1 Typical chromatogram of dimethylamine aqueous solution
A2 Chromatographic operating conditions
Column temperature: 50℃, vaporization chamber temperature=detection temperature=130℃;
Carrier gas (H 2 ) flow rate: 60mL/min;
Bridge current: 150mA;
Injection volume: 2uL;
Paper speed: 30cm/h;
Chromatographic column: φ3 mm(id)×2m stainless steel column;
Carrier: 201 red carrier;
Fixing solution: cetyl alcohol , polyethylene glycol 600, potassium hydroxide