 Home > Chemicals Industry > Chemical Technology > Product standard for the process flow of ethyl chloroacetate

Product standard for the process flow of ethyl chloroacetate

 Last Update: 2021-08-14
 Source: Internet
 Author: User

Tags

amodimethicone water soluble

liquid nitrogen storage tank

Search more information of high quality chemicals, good prices and reliable suppliers, visit www.echemi.com

Ethyl chloroacetate (chloroacetic acid ethyl ester), also known as ethyl chloroacetate, has a molecular formula of C ₄ H ₇ CIO ₂ , a molecular weight of 122.
55, and a structural formula of

Product performance

Colorless and transparent liquid; flammable; highly toxic; steam has anesthetic effect, irritating eyes, skin and mucous membranes, and damages the liver and blood; insoluble in water, soluble in ethanol , ether and benzene; in hot water and Easy to decompose in alkali; freezing point -26℃; boiling point 145～146℃, 52℃ (2.
67kPa), relative density (d ₄²⁰ ) 1.
1585, refractive index (n _D²⁰ ) 1.
4227, flash point 54℃
.

2.
Production principle

It is obtained by direct esterification of chloroacetic acid and absolute ethanol
.

Process flow

Technical formula (kg/t)

Main equipment

Esterification reactor, fractionation column, ethanol storage tank, distillation kettle (vacuum pump)
.

6.
Production process

Put 950 kg of chloroacetic acid and 217 kg of anhydrous ethanol into the esterification reactor, and heat to reflux with stirring.
At the same time, the by-product water is separated through a fractionating column and the ethanol is distilled out
.

After refluxing for 2 hours, 217 kg of absolute ethanol and the distilled ethanol were added to perform the second reflux reaction

7.
Product Standard

Product use

Used as a synthetic raw material for medicine and perfume, also used in organic synthesis, and can also be used as a solvent
.

9.
Safety measures

(1) The chloroacetic acid used in the production is an organic drug, which is a secondary organic acid corrosive substance, and anhydrous ethanol is flammable
.

The equipment should be sealed to prevent leakage, the operator should wear labor protection equipment, and pay attention to ventilation and fire prevention in the workshop

(2) This product is toxic and flammable
.

Packed in glass bottles and stored in a cool, dry place

Related links: Product performance and production principle of urethane

This article is an English version of an article which is originally in the Chinese language on echemi.com and is provided for information purposes only. This website makes no representation or warranty of any kind, either expressed or implied, as to the accuracy, completeness ownership or reliability of the article or any translations thereof. If you have any concerns or complaints relating to the article, please send an email, providing a detailed description of the concern or complaint, to service@echemi.com. A staff member will contact you within 5 working days. Once verified, infringing content will be removed immediately.

Related Products

1-Octanol 111-87-5

CAS No.: 111-87-5

Industrial Grade

$1944/MT FOB

BHT- free polyether polyol, hot selling with after-sale service guaranteed, MW 6000 polyol

CAS No.: 9082-00-2

Industrial Grade

$1445-1475/MT FOB

Lithium-ion Batteries PVDF Resin with remarkable electrochemical stability

CAS No.: 24937-79-9

Chemical Grade

$40/KG FOB

Hot Tags

united states jobs(223)

jobs united states(236)

1 year treasury(277)

1 year subscription(296)

announcements today(81)

80 20 company(94)

united states logo(227)

single use technology(195)

healthy food name(42)

ups united states(221)

Hot Articles

The source of this page with content of products and services is from Internet, which doesn't represent ECHEMI's opinion. If you have any queries, please write to service@echemi.com. It will be replied within 5 days.

Moreover, if you find any instances of plagiarism from the page, please send email to service@echemi.com with relevant evidence.