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M-aminobenzoic acid (m-aminobenzoic acid), also known as 3-aminobenzoic acid, of the formula C .
7 H .
7 NO 2 , a molecular weight of 137.
14, the formula
1.
Product performance
White or light yellow crystals; melting point 174℃; relative density (d 4 20 ) 1.
5105; slightly soluble in cold water, cold alcohol and cold chloroform, soluble in acetone , soluble in boiling water, hot ethanol, hot chloroform and ether , insoluble in benzene , Gasoline; sweet, sublimable, but partially decomposed; toxic; acidic and corrosive
.
2.
Production principle
1) Catalytic hydrogenation method
Meta-nitrobenzoic acid is catalyzed by palladium-carbon and hydrogen-catalyzed reduction to obtain meta-aminobenzoic acid
.
2) Iron powder reduction method
M-nitrobenzoic acid is reduced with iron powder in acid medium to obtain m-aminobenzoic acid
.
3.
Process flow
1) Catalytic hydrogenation method
2) Iron powder reduction method
4.
Technical formula
5.
Main equipment
1) Catalytic hydrogenation method
Dissolving and decolorizing kettle, hydrogenation kettle, filter, acidification kettle, dryer
2) Iron powder reduction method
Reduction kettle, plate and frame filter press, acidification pot, vacuum filter, storage tank, dryer
Related links: Isophthalic acid product performance and production principle