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[Structural formula]
[Physical and chemical properties] Rosinamine is a light yellow viscous oily liquid
Slightly soluble in boiling water (0.
[Preparation]
(1) High pressure hydrogenation method
From rosin nitrile, rosin amine is prepared by catalytic hydrogenation under high temperature and high pressure
The catalytic hydrogenation of rosin nitrile is a heterogeneous catalytic exothermic reaction, using skeleton nickel as a catalyst, a small amount of sodium hydroxide as a promoter, and ethanol as a solvent
The rate of the hydrogenation reaction depends on the pressure of hydrogen and the activity of the catalyst
Industrially, 20kg of rosin nitrile, 38kg of industrial ethanol , 6kg of nickel, and 200g of sodium hydroxide are used and mixed and stirred evenly
(2) Rosin melting method
The ingredient ratio is disproportionated rosin: ammonia: red phosphorus: boric acid = 1: 0.
[Technical Index] Enterprise Standard Jilin Chemical Plant Commodity
[Application] Rosin amine is generally packed in iron drums