UV Identification of Baoxin Tablets, Paper Chromatography Identification of Huazheng Huisheng Tablets and TLC Identification of Niuhuang Jiedu Pills

UV identification of Baoxin tablets

[Prescription] Panax notoginseng 45g Danshen 540g Chuanxiong 360g Hawthorn 450g Polygonum multiflorum 157.

[Identification] Take 1 piece of this product, grind it into fine pieces, add water and stir to dissolve, filter, take 1ml of the filtrate, add water to 25ml, and shake well

Identification of Huazheng Huisheng Tablets by Paper Chromatography

[Prescription] Motherwort 112g Safflower 14g Pepper (charcoal) 14g Hot leech 14g Angelica 28g Hematoxylin 14g

Vinegar Triangular 14g Two Tips 14g Chuanxiong 14g Dalbergia 14g Vinegar Fragrant 14g Ginseng 42g Galangal 14g

Turmeric.

Salt cumin 21g, peach kernel 21g, Wulingzhi (vinegar broiled) 14g, horsefly 14g

Turtle Glue 112g Clove 21g Vinegar Corydalis 14g White Peony 28g

Cattail yellow charcoal 14g Frankincense (vinegar broiled) 14g Dry paint (calcined) 14g Evodia 14g

Asafoetida 14g Cinnamon 14 Vinegar Moxa Charcoal 14g Rehmannia glutinosa 28g Perilla Seed 14g

[Identification] Take 20 tablets of this product, grind it into fine pieces, add 50ml of 80% ethanol, heat to reflux for 1 hour, filter, and evaporate the filtrate to dryness, add 5ml of 1% hydrochloric acid solution to the residue to dissolve, filter, and add sodium carbonate test solution to the filtrate dropwise Adjust the pH to 8, filter, evaporate the filtrate, add 3ml 80% ethanol to the residue to dissolve it, and use it as the test solution

TLC Identification of Niuhuang Jiedu Pills

[Prescription] Artificial Bezoar 5g Realgar 50g Plaster 200g Rhubarb 200g

Scutellaria 150g Platycodon grandiflorum 100g Borneol 25g Licorice 50g

[Identification] Take 3g of this product water honey pill, cut into pieces, or take 3g of big honey pill, cut into pieces, add 2g of diatomaceous earth, grind well, add 15ml of chloroform, sonicate for 20 minutes, filter, filter the residue and evaporate the solvent Add 30ml of methanol, sonicate for 20 minutes, filter, evaporate the solvent, add 30ml of methanol , sonicate for 20 minutes, filter, take 5ml of the filtrate, evaporate to dryness, add 10ml of water to the residue to dissolve, add 1ml of hydrochloric acid, and place in a water bath Heat for 30 minutes, cool immediately, shake and extract 4 times with ether , 10ml each time, combine the ether solution, evaporate to dryness, add 1ml ethyl acetate to the residue to dissolve, as the test solution

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