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Bis(1,2,2,6,6-pentamethyl-4-piperidyl) decanedioate is a synthetic chemical compound that is commonly used in a variety of applications, including as a fragrance ingredient, as a solvent, and as an interviewing agent.
The production process for this compound involves a number of steps, including the preparation of the starting materials, the reaction of the starting materials to form the bis(1,2,2,6,6-pentamethyl-4-piperidyl) decanedioate, and the purification and isolation of the final product.
The first step in the production process for bis(1,2,2,6,6-pentamethyl-4-piperidyl) decanedioate is the preparation of the starting materials.
This typically involves the synthesis of the compound known as N-pentyl-N-methylpiperidine-2,4-diamine and the compound known as decanal.
N-pentyl-N-methylpiperidine-2,4-diamine is synthesized by reacting N-methylpiperidine with N-pentylamine in the presence of a catalyst, such as hydrochloric acid.
Decanal is synthesized by the reduction of decylbenzene using a reducing agent, such as sodium in powdered zinc.
Once the starting materials have been prepared, the next step in the production process is the reaction of the starting materials to form bis(1,2,2,6,6-pentamethyl-4-piperidyl) decanedioate.
This reaction is typically carried out in the presence of a solvent, such as ethyl ether, and a condensing agent, such as hydrochloric acid.
The reaction is typically performed under conditions of heat and pressure, and the resulting product is purified and isolated by recrystallization.
The final step in the production process for bis(1,2,2,6,6-pentamethyl-4-piperidyl) decanedioate is the purification and isolation of the final product.
This typically involves the dissolution of the crude product in a solvent, such as ethyl acetate, and the subsequent removal of the solvent by distillation.
The resulting crystalline product is then collected and dried to remove any remaining impurities.
Overall, the production process for bis(1,2,2,6,6-pentamethyl-4-piperidyl) decanedioate involves a number of steps, including the preparation of the starting materials, the reaction of the starting materials to form the desired product, and the purification and isolation of the final product.
This compound is commonly used in a variety of applications and is an important component in the production of a wide range of chemical products.