echemi logo
  • Product
  • Supplier
  • Inquiry
    Home > Organic Chemistry Topics > Organic Chemistry Products News > The Production Process of TRI-TERT-BUTYL 1 4 7 10-TETRAAZACYCLONONANE

    The Production Process of TRI-TERT-BUTYL 1 4 7 10-TETRAAZACYCLONONANE

    • Last Update: 2023-04-29
    • Source: Internet
    • Author: User
    Search more information of high quality chemicals, good prices and reliable suppliers, visit

    TRI-TERT-BUTYL 1,4,7,10-TETRAAZACYCLONONANE, also known as TBTN, is an organic compound used as a catalyst in various chemical reactions.
    The production process of TBTN involves several steps, which are outlined below.

    Step 1: Preparation of the Starting Materials

    The production of TBTN starts with the preparation of the starting materials.
    These materials include tert-butyl chloride and sodium azide.
    Tert-butyl chloride is prepared by reacting tert-butyl alcohol with hydrogen chloride gas, while sodium azide is prepared by the reaction of sodium amide with hydrogen azide.

    Step 2: Condensation Reaction

    The next step in the production of TBTN is the condensation reaction between tert-butyl chloride and sodium azide.
    This reaction is carried out in the presence of a solvent, such as ether or hexane, and a catalyst, such as sodium hydroxide or hydrochloric acid.
    The condensation reaction leads to the formation of TBTN, which is a colorless liquid with a distinctive odor.

    Step 3: Purification of TBTN

    After the condensation reaction, the TBTN produced is typically impure and contains impurities such as tert-butanol and sodium chloride.
    To purify TBTN, the liquid is typically filtered to remove any solid impurities, and then the liquid is distilled to separate the various components.
    The TBTN is then collected and used as a catalyst in further chemical reactions.

    Step 4: Storage and Handling

    TBTN is a sensitive and hazardous material, and proper storage and handling precautions must be taken to prevent accidents or environmental contamination.
    TBTN should be stored in a cool, dry place and handled with care to avoid any spills or leaks.
    It is also important to wear appropriate personal protective equipment (PPE), such as gloves and safety glasses, when handling TBTN.

    In conclusion, the production process of TBTN involves several steps, including the preparation of starting materials, the condensation reaction, purification of the TBTN, and storage and handling.
    TBTN is an important catalyst in various chemical reactions and is used in the production of a wide range of chemical products.
    However, it is important to handle TBTN with care due to its sensitivity and potential hazards.

    This article is an English version of an article which is originally in the Chinese language on and is provided for information purposes only. This website makes no representation or warranty of any kind, either expressed or implied, as to the accuracy, completeness ownership or reliability of the article or any translations thereof. If you have any concerns or complaints relating to the article, please send an email, providing a detailed description of the concern or complaint, to A staff member will contact you within 5 working days. Once verified, infringing content will be removed immediately.

    Contact Us

    The source of this page with content of products and services is from Internet, which doesn't represent ECHEMI's opinion. If you have any queries, please write to It will be replied within 5 days.

    Moreover, if you find any instances of plagiarism from the page, please send email to with relevant evidence.