The Synthetic Routes of 7-Amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid diphenylmethyl ester hydrochloride

Introduction

7-Amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid diphenylmethyl ester hydrochloride is a synthetic compound that has been widely used in the chemical industry for various purposes.
This compound is a derivative of the naturally occurring compound, 7-amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid, which is found in certain plants and bacteria.

Synthesis of 7-Amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid diphenylmethyl ester hydrochloride

The synthesis of 7-Amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid diphenylmethyl ester hydrochloride involves several steps, including the preparation of the starting materials, the reaction steps, and the purification of the final product.

Preparation of starting materials

The synthesis of 7-Amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid diphenylmethyl ester hydrochloride requires the preparation of several starting materials, including 7-amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid, which is isolated from certain plants and bacteria, and diphenylmethyl ester, which is synthesized using commercially available reagents.

Reaction steps

Once the starting materials are prepared, the next step is to synthesize the target compound.
This involves a series of chemical reactions, including the condensation of the starting materials to form the diphenylmethyl ester derivative of 7-amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid.
The reaction is carried out in the presence of a solvent, such as toluene, and a catalyst, such as pyridine, to accelerate the reaction.

Purification of the final product

After the reaction is complete, the final product is obtained as a mixture of the desired compound and other byproducts.
To purify the final product, the mixture is subjected to a series of chromatographic techniques, such as precipitation, crystallization, and high-performance liquid chromatography (HPLC).
These techniques are used to separate the desired compound from the byproducts and to obtain a pure sample for further use.

Properties and uses of 7-Amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid diphenylmethyl ester hydrochloride

7-Amino-8-oxo-3-(cis-prop-1-enyl)-5-thia-1-azabicyclo[4.
2.
0]oct-2-ene-2-carboxylic acid diphenylmeth